Part 261 Identification and Listing of Hazardous Waste Appendices
Appendix I - Representative Sampling Methods
The methods and equipment used for sampling waste materials will vary with the form and consistency of the waste materials to be sampled. Samples collected using the sampling protocols listed below, for sampling waste with properties similar to the indicated materials, will be considered by the Department to be representative of the waste.
Extremely viscous liquid - ASTM Standard D140-70 Crushed or powdered material - ASTM Standard D346-75 Soil or rock-like material - ASTM Standard D420-89 Soil-like material - ASTM Standard D1452-65
Fly Ash-like material - ASTM Standard D2234-76 [ASTM Standards are available from ASTM, 1916 Race St., Philadelphia, PA 19103]
Containerized liquid wastes - "COLIWASA" described in "Test Methods for the Evaluation of Solid Waste, Physical/Chemical Methods," U.S. Environmental Protection Agency, WH-5658 Office of Solid Waste, Washington, D.C. 20460
Liquid waste in pits, ponds, lagoons, and similar reservoirs - "Pond Sampler" described in "Test Methods for the Evaluation of Solid Waste, Physical/Chemical Methods(1)."
The manual also contains additional information on application of these protocols.
_________________
(1) The methods are also described in "Samplers and Sampling Procedures for Hazardous Waste Streams," EPA 600/2-80-018, January 1980.
Appendix II - Method 1311 Toxicity Characteristic Leaching Procedure (TCLP)
Note: The TCLP (Method 1311) is published in "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods," EPA Publication SW-846, as incorporated by reference in §260.11 of these regulations.
Appendix III - Chemical Analysis Test Methods
Note: Appropriate analytical procedures to determine whether a sample contains a given toxic constituent are specified in Chapter Two, "Choosing the Correct Procedure" found in "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods," EPA Publication SW-846, as incorporated by reference in §260.11 of these regulations. Prior to final sampling and analysis method selection, the individual should consult the specific section or method described in SW-846 for additional guidance on which of the approved methods should be employed for a specific sample analysis situation.
(Amended July 23, 1996)
Appendix IV - [Reserved for Radioactive Waste Test Methods]
Appendix V - [Reserved for Infectious Waste Treatment Specifications]
Appendix VI - [Reserved for Etiologic Agents]
Appendix VII - Basis for Listing Hazardous Waste
_______________________________________________________________________________
EPA hazardous waste No. |
Hazardous constituents for which listed |
F001 F002 F003 F004 F005 F006 F007 F008 F009 F010 F011 F012 F019 F020 F021 F022 F023 F024 F025 F026 F027 F028 F032 F034 F035 F037 F038 F039 K001 K002 K003 K004 K005 K006 K007 K008 K009 K010 K011 K013 K014 K015 K016 K017 K018 K019 K020 K021 K022 K023 K024 K025 K026 K027 K028 K029 K030 K031 K032 K033 K034 K035 K036 K037 K038 K039 K041 K042 K043 K044 K045 K046 K047 K048 K049 K050 K051 K052 K060 K061 K062 K064 K065 K066 K069 K071 K073 K083 K084 K085 K086 K087 K088 K090 K091 K093 K094 K095 K096 K097 K098 K099 K100 K101 K102 K103 K104 K105 K106 K107 K108 K109 K110 K111 K112 K113 K114 K115 K116 K117 K118 K123 K124 K125 K126 K131 K132 K136 K141 K142 K143 K144 K145 K147 K148 K149 K150 K151 K156 K157 K158 K159 K161 K169 K170 K171 K172 K174 K175 K176 K177 K178 |
Tetrachloroethylene, methylene chloride trichloroethylene, 1,1,1-trichloroethane, carbon tetrachloride, chlorinated fluorocarbons. Tetrachloroethylene, methylene chloride, trichloroethylene, 1,1,1-trichloroethane, 1,1,2-trichloroethane, chlorobenzene, 1,1,2-trichloro-1,2,2-trifluoroethane, ortho-dichlorobenzene, trichlorofluoromethane. N.A. Cresols and cresylic acid, nitrobenzene. Toluene, methyl ethyl ketone, carbon disulfide, isobutanol, pyridine, 2-ethoxyethanol, 2-nitropropane. Cadmium, hexavalent chromium, nickel, cyanide (complexed). Cyanide (salts). Cyanide (salts). Cyanide (salts). Cyanide (salts). Cyanide (salts). Cyanide (complexed). Hexavalent chromium, cyanide (complexed). Tetra- and pentachlorodibenzo-p-dioxins; tetra and pentachlorodi-benzofurans; tri- and tetrachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. Penta- and hexachlorodibenzo-p-dioxins; penta- and hexachlorodibenzofurans; pentachlorophenol and its derivatives. Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra-, penta-, and hexachlorodibenzofurans. Tetra-, and pentachlorodibenzo-p-dioxins; tetra- and pentachlorodibenzofurans; tri- and tetrachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. Chloromethane, dichloromethane, trichloromethane, carbon tetrachloride, chloroethylene, 1-dichloroethane, 1,2-dichloroethane, trans-1-2-dichloroethylene, 1,1-dichloroethylene, 1,1,1-trichloroethane, 1,1,2-trichloroethane, trichloroethylene, 1,1,1,2-tetra-chloroethane, 1,1,2,2-tetrachloroethane, tetrachloroethylene, pentachloroethane, hexachloroethane, allyl chloride (3-chloropropene), dichloropropane, dichloropropene, 2-chloro-1,3-butadiene, hexachloro-1,3-butadiene, hexachlorocyclopentadiene, hexachlorocyclohexane, benzene, chlorbenzene, dichlorobenzenes, 1,2,4-trichlorobenzene, tetrachlorobenzene, pentachlorobenzene, hexachlorobenzene, toluene, naphthalene. Chloromethane; Dichloromethane; Trichloromethane; Carbontetrachloride; Chloroethylene; 1,1-Dichloroethane; 1,2-Dichloroethane; trans-1,2-Dichloroethylene; 1,1-Dichloroethylene; 1,1,1-Trichloroethane; 1,1,2-Trichloroethane; Trichloroethylene; 1,1,1,2-Tetrachloroethane; 1,1,2,2-Tetrachloroethane; Tetrachloroethylene; Pentachloroethane; Hexachloroethane; Allyl chloride (3-Chloropropene); Dichloropropane; Dichloropropene; 2-Chloro-1,3-butadiene; Hexachloro-1,3-butadiene; Hexachlorocyclopentadiene; Benzene; Chlorobenzene; Dichlorobenzene; 1,2,4-Trichloro- benzene; Tetrachlorobenzene; Pentachlorobenzene; Hexachlorobenzene; Toluene; Naphthalene. Tetra- and pentachlorodibenzo-p-dioxins; tetra and pentachlorodi-benzofurans; tri- and tetrachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra-, penta-, and hexachlorodibenzofurans; tri-, tetra-, and pentachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. Tetra-, penta-, and hexachlorodibenzo-p-dioxins; tetra-, penta-, and hexachlorodibenzofurans; tri-, tetra-, and pentachlorophenols and their chlorophenoxy derivative acids, esters, ethers, amine and other salts. Benz(a)anthracene, benzo(a)pyrene, dibenz(a,h)- anthracene, indeno(1,2,3-cd)pyrene, pentachlorophenol, arsenic, chromium, tetra-, penta-, hexa-, heptachlorodibenzo-p-dioxins, tetra-, penta-, hexa-, heptachlorodibenzofurans. Benz(a)anthracene, benzo(k)fluoranthene, benzo(a)pyrene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene, naphthalene, arsenic, chromium. Arsenic, chromium, lead. Benzene, benzo(a)pyrene, chrysene, lead, chromium. Benzene, benzo(a)pyrene, chrysene, lead, chromium. All constituents for which treatment standards are specified for multi-source leachate (wastewaters and nonwastewaters) under section 268.43, Table CCW, of these regulations. Pentachlorophenol, phenol, 2-chlorophenol, p-chloro-m-cresol, 2,4-dimethylphenyl, 2,4-dinitrophenol, trichlorophenols, tetrachlorophenols, 2,4-dinitrophenol, creosote, chrysene, naphthalene, fluoranthene, benzo(b)fluoranthene, benzo(a)pyrene, indeno(1,2,3-cd)pyrene, benz(a)anthracene, dibenz(a)anthracene, acenaphthalene. Hexavalent chromium, lead Hexavalent chromium, lead. Hexavalent chromium. Hexavalent chromium, lead. Hexavalent chromium. Cyanide (complexed), hexavalent chromium. Hexavalent chromium. Chloroform, formaldehyde, methylene chloride, methyl chloride, paraldehyde, formic acid. Chloroform, formaldehyde, methylene chloride, methyl chloride, paraldehyde, formic acid, chloroacetaldehyde. Acrylonitrile, acetonitrile, hydrocyanic acid. Hydrocyanic acid, acrylonitrile, acetonitrile. Acetonitrile, acrylamide. Benzyl chloride, chlorobenzene, toluene, benzotrichloride. Hexachlorobenzene, hexachlorobutadiene, carbon tetrachloride, hexachloroethane, perchloroethylene. Epichlorohydrin, chloroethers [bis(chloromethyl) ether and bis (2-chloroethyl) ethers], trichloropropane, dichloropropanols. 1,2-dichloroethane, trichloroethylene, hexachlorobutadiene, hexachlorobenzene. Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane, tetrachloroethanes (1,1,2,2-tetrachloroethane and 1,1,1,2-tetrachloroethane), trichloroethylene, tetrachloroethylene, carbon tetrachloride, chloroform, vinyl chloride, vinylidene chloride. Ethylene dichloride, 1,1,1-trichloroethane, 1,1,2-trichloroethane, tetrachloroethanes(1,1,2,2-tetrachloroethane and 1,1,1,2-tetrachloroethane), trichloroethylene, tetrachloroethylene, carbon tetrachloride, chloroform, vinyl chloride, vinylidene chloride. Antimony, carbon tetrachloride, chloroform. Phenol, tars (polycyclic aromatic hydrocarbons). Phthalic anhydride, maleic anhydride. Phthalic anhydride, 1,4-naphthoquinone. Meta-dinitrobenzene, 2,4-dinitrotoluene. Paraldehyde, pyridines, 2-picoline. Toluene diisocyanate, toluene-2, 4-diamine. 1,1,1-trichloroethane, vinyl chloride. 1,2-dichloroethane, 1,1,1-trichloroethane, vinyl chloride, vinylidene chloride, chloroform. Hexachlorobenzene, hexachlorobutadiene, hexachloroethane, 1,1,1,2-tetrachloroethane, 1,1,2,2-tetrachloroethane, ethylene dichloride. Arsenic. Hexachlorocyclopentadiene. Hexachlorocyclopentadiene. Hexachlorocyclopentadiene. Creosote, chrysene, naphthalene, fluoranthene benzo(b) fluoranthene, benzo(a)pyrene, indeno(1,2,3-cd) pyrene, benzo(a)anthracene, dibenzo(a)anthracene, acenaphthalene. Toluene, phosphorodithioic and phosphorothioic acid esters. Toluene, phosphorodithioic and phosphorothioic acid esters. Phorate, formaldehyde, phosphorodithioic and phosphorothioic acid esters. Phosphorodithioic and phosphorothioic acid esters. Phorate, formaldehyde, phosphorodithioic and phosphorothioic acid esters. Toxaphene. Hexachlorobenzene, ortho-dichlorobenzene. 2,4-dichlorophenol, 2,6-dichlorophenol, 2,4,6-trichlorophenol. N.A. N.A. Lead. N.A. Hexavalent chromium, lead. Hexavalent chromium, lead. Hexavalent chromium. Hexavalent chromium, lead. Lead. Cyanide, napthalene, phenolic compounds, arsenic. Hexavalent chromium, lead, cadmium. Hexavalent chromium, lead. Lead, cadmium. Do. Do. Hexavalent chromium, lead, cadmium. Mercury. Chloroform, carbon tetrachloride, hexachloroethane, trichloroethane, tetrachloroethylene, dichloroethylene, 1,1,2,2-tetrachloroethane. Aniline, diphenylamine, nitrobenzene, phenylenediamine. Arsenic. Benzene, dichlorobenzenes, trichlorobenzenes, tetrachlorobenzenes, pentachlorobenzene, hexachlorobenzene, benzyl chloride. Lead, hexavalent chromium. Phenol, naphthalene. Cyanide (complexes). Chromium. Do. Phthalic anhydride, maleic anhydride. Phthalic anhydride. 1,1,2-trichloroethane, 1,1,1,2-tetrachloroethane, 1,1,2,2-tetrachloroethane. 1,2-dichloroethane, 1,1,1-trichloroethane,1,1,2-trichloroethane. Chlordane, heptachlor. Toxaphene. 2,4-dichlorophenol, 2,4,6-trichlorophenol. Hexavalent chromium, lead, cadmium. Arsenic. Arsenic. Aniline, nitrobenzene, phenylenediamine. Aniline, benzene, diphenylamine, nitrobenzene, phenylenediamine Benzene, monochlorobenzene, dichlorobenzenes, 2,4,6-trichlorophenol Mercury 1,1-Dimethylhydrazine (UDMH) 1,1-Dimethylhydrazine(UDMH) 1,1-Dimethylhydrazine (UDMH) 1,1-Dimethylhydrazine(UDMH) 2,4-Dinitrotoluene 2,4-Toluenediamine, o-toluidine, p-toluidine, aniline 2,4-Toluenediamine, o-toluidine, p-toluidine, aniline 2,4-Toluenediamine, o-toluidine, p-toluidine 2,4-Toluenediamine Carbon tetrachloride, tetrachloroethylene chloroform, phosgene Ethylene dibromide Ethylene dibromide Ethylene thiourea Ethylene thiourea Ethylene thiourea Ethylene thiourea Dimethyl sulfate, methyl bromide Methyl bromide Ethylene dibromide Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene. Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene. Benzene, benz(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene. Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene. Benzene, benz(a)anthracene, benzo(a)pyrene, dibenz(a,h)anthracene, naphthalene. Benzene, benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene. Benz(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene. Benzotrichloride, benzyl chloride, chloroform, chloromethane, chlorobenzene, 1,4-dichlorobenzene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5-tetrachlorobenzene, toluene. Carbon tetrachloride, chloroform, chloromethane, 1,4-dichlorobenzene, hexachlorobenzene, pentachlorobenzene, 1,2,4,5-tetrachlorobenzene, 1,1,2,2-tetrachloroethane, tetrachloroethylene, 1,2,4-trichlorobenzene. Benzene, carbon tetrachloride, chloroform, hexachlorobenzene, pentachlorobenzene, toluene, 1,2,4,5-tetrachlorobenzene, tetrachloroethylene. Benomyl, carbaryl, carbendazim, carbofuran, carbosulfan, formaldehyde, methylene chloride, triethylamine. Carbon tetrachloride, formaldehyde, methyl chloride, methylene chloride, pyridine, triethylamine. Benomyl, carbendazim, carbofuran, carbosulfan, chloroform, methylene chloride. Benzene, butylate, eptc, molinate, pebulate, vernolate. Antimony, arsenic, metam-sodium, ziram. Benzene. Benzo(a)pyrene, dibenz(a,h)anthracene, benzo(a)anthracene, benzo(b)fluoranthene, benzo(k)fluoranthene, 3-methylcholanthrene, 7,12-demethylbenz(a)anthracene. Benzene, arsenic. Benzene, arsenic. 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-HpCDD), 1,2,3,4,6,7,8- Heptachlorodibenzofuran (1,2,3,4,6,7,8-HpCDF), 1,2,3,4,7,8,9-Heptachlorodibenzofuran (1,213,6,7,8,9-HpCDF), HxCDDs (All Hexachlorodibenzo-p-dioxins), HxCDFs (All Hexachlorodibenzofurans), PeCDDs (All Pentachlorodibenzo-p-dioxins), OCDD (1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin), OCDF (1,2,3,4,6,7,8,9-Octachlorodibenzofuran), PeCDFs (All Pentachlorodibenzofurans), TCDDs (All Tetrachlorodibenzo-p-dioxins), TCDFs (All Tetrachlorodibenzofurans). Mercury. Arsenic, Lead. Antimony. Thallium. |
N.A. - Waste is hazardous because it fails the test for the characteristic of ignitability, corrosivity, or reactivity.
(Amended February 5, 1985; November 21, 1985; May 8, 1986; August 29, 1988; August 10, 1990; June 19, 1992, August 1, 1995, August 21, 1997, January 1, 1999, August 23, 1999, April 23, 2001, July 1, 2002, August 21, 2006)
Common Name |
Chemical Abstracts Name |
Chemical Abstracts Number |
Haz. Waste # |
A2213 |
Ethanimidothioic acid, 2- (dimethylamino) -N-hydroxy-2-oxo-, methyl ester |
30558-43-1 |
U394 |
Acetonitrile |
Same |
75-05-8 |
U003 |
Acetophenone |
Ethanone, 1-phenyl- |
98-86-2 |
U004 |
2-Acetylaminefluarone |
Acetamide, N-9H-fluoren-2-yl- |
53-96-3 |
U005 |
Acetyl chloride |
Same |
75-36-5 |
U006 |
1-Acetyl-2-thiourea |
Acetamide, N-(aminothioxomethyl)- |
591-08-2 |
P002 |
Acrolein |
2-Propenal |
107-02-8 |
P003 |
Acrylamide |
2-Propenamide |
79-06-1 |
U007 |
Acrylonitrile |
2-Propenenitrile |
107-13-1 |
U009 |
Aflatoxins |
Same |
1402-68-2 |
|
Aldicarb |
Propanal, 2-methyl-2-(methylthio)-, O-[(methylamino)carbonyl]oxime |
116-06-3 |
P070 |
Aldicarb sulfone |
Propanal, 2-methyl-2- (methylsulfonyl) -, 0-[(methylamino) carbonyl] oxime |
1646-88-4 |
P203 |
Aldrin |
1,4,5,8-Dimethanonaphthalene, 1,2,3,4,10,10-10-hexachloro-1,4,4a,5,8,8a-hexahydro-, (1alpha,4alpha,4abeta,5alpha,8alpha, 8abeta)- |
309-00-2 |
P004 |
Allyl alcohol |
2-Propen-1-ol |
107-18-6 |
P005 |
Allyl chloride |
1-Propane, 3-chloro |
107-05-1 |
|
Aluminum phosphide |
Same |
20859-73-8 |
P006 |
4-Aminobiphenyl |
[1,1'-Biphenyl]-4-amine |
92-67-1 |
|
5-(Aminomethyl)-3-isoxazolol |
3(2H)-Isoxazolone, 5-(aminomethyl)- |
2763-96-4 |
P007 |
4-Aminopyridine |
4-Pyridinamine |
504-24-5 |
P008 |
Amitrole |
1H-1,2,4-Triazol-3-amine |
61-82-5 |
U011 |
Ammonium vanadate |
Vanadic acid, ammonium salt |
7803-55-6 |
P119 |
Aniline |
Benzenamine |
62-53-3 |
U012 |
o-Anisidine (2-methoxyaniline) |
Benzenamine, 2-Methoxy- |
90-04-0 |
|
Antimony |
Same |
7440-36-0 |
|
Antimony compounds, N.O.S.1 |
|||
Aramite |
Sulfurous acid, 2-chloroethyl 2-[4-(1,1-dimethylethyl)phenoxy]-1-methylethyl ester |
140-57-8 |
|
Arsenic |
Same |
7440-38-2 |
|
Arsenic compounds, N.O.S.1 |
|||
Arsenic acid |
Arsenic acid H3AsO4 |
7778-39-4 |
P010 |
Arsenic pentoxide |
Arsenic oxide As2O5 |
1303-28-2 |
P011 |
Arsenic trioxide |
Arsenic oxide As2O3 |
1327-53-3 |
P012 |
Auramine |
Benzenamine, 4,4'-carbonimidoylbis[N,N-dimethyl |
492-80-8 |
U014 |
Azaserine |
L-Serine, diazoacetate (ester) |
115-02-6 |
U015 |
Barban |
Carbamic acid, (3-chlorophenyl)-, 4-chloro-2-butynyl ester |
101-27-9 |
U280 |
|
Barium |
Same |
7440-39-3 |
|
Barium compounds, N.O.S.1 |
|||
Barium cyanide |
Same |
542-62-1 |
P013 |
Bendiocarb |
1,3-Benzodioxol-4-ol, 2,2-dimethyl-, methyl carbamate |
22781-23-3 |
U278 |
Bendiocarb phenol |
1,3-Benzodioxol-4-ol, 2,2-dimethyl-, |
22961-82-6 |
U364 |
Benomyl |
Carbamic acid, [1- [(butylamino) carbonyl]- 1H-benzimidazol-2-yl] -, methyl ester |
17804-35-2 |
U271 |
Benz[c]acridine |
Same |
225-51-4 |